TRIFLUOROMETHANESULFONAMIDE Me CAS 421-85-2

CAS:421-85-2

MF:CH2F3NO2S

MW:149.09

EINECS No:431-270-1

Nā huaʻōlelo like:Trifluoromethanesulfonamide 96%; trifluoromethylsulfonamide; Trifluoromethanesulphonamide 98%; Trifluoromethanesulphonami 98%; Trifluoromethanesulfonimidicacid; TrifluoroMethanesulfonaMide 95%; TRIFLAMIDE

Waiho i kāu leka

Huahana Huahana

Hoʻoiho

Huahana Huahana

He aha ka TRIFLUOROMETHANESULFONAMIDE Me CAS 421-85-2?

ʻO Trifluoromethanesulfonamide kahi mea hoʻohui kūlohelohe, hiki ke hoʻomākaukau ʻia e ka hopena o ka trifluoromethanesulfonyl chloride a me ke kinoea amonia. Hiki ke hoʻohana ʻia ka Trifluoromethanesulfonyl e hoʻomākaukau i ka LiTFSI. ʻO LiTFSI kahi mea hoʻohui electrolyte organik maikaʻi loa no nā pā lithium. Ma muli o ke ʻano kemika kūikawā o ka ʻāpana anion (CF3SO2) 2N-, loaʻa i ka LiTFSI ke kūpaʻa electrochemical kiʻekiʻe a me ka conductivity uila; Hoʻohālikelike ʻia me LiClO4 a me LiPF6, LiTFSI e like me ka mea hoʻohui electrolyte hiki ke: 1) hoʻomaikaʻi i ke kiʻi SEI o nā electrodes maikaʻi a maikaʻi ʻole; 2) hoʻopaʻa i ka pilina o nā electrodes maikaʻi a maikaʻi ʻole; 3) kaohi i ka hana kinoea; 4) hoʻomaikaʻi i ka hana pōʻaiapuni; 5) hoʻomaikaʻi i ke kūpaʻa wela kiʻekiʻe; 6) E hoʻomaikaʻi i ka hana mālama a me nā pono ʻē aʻe.

Hōʻike

'ikamu	Kūlana
Ka nana aku	Paʻa kalakala keʻokeʻo
Hoʻāʻo	≥98%
Māmā	≤0.50%

Palapala noi

E hoʻohui i 172g o 98% CF3SO2Cl (1mol) a me 500mL o anhydrous acetonitrile ma hope o ka mālama ʻana i ka wai i loko o kahi reactor pani ʻia me kahi thermometer, kahi mea hoʻoulu, a me ka wehe ʻana o ka nitrogen a me ka oxygen. Hoʻokiʻekiʻe mālie ʻia ke kinoea amonia a i ʻole ka nui like o ka ammonium carbonate maloʻo i ka lumi wela ma lalo o ka hoʻoulu ʻana, a hoʻopau ʻia ka hopena ma hope o 3 mau hola o ka hopena. Ua wehe ʻia ka ammonium chloride i loko o ka hopena hopena ma ka kānana ʻana, ua hoʻoheheʻe ʻia ka mea hoʻoheheʻe i loko o ka filtrate ma lalo o ke kaomi hoʻemi ʻia, a hoʻomaloʻo ʻia ma lalo o ke kaomi hoʻemi ʻia ma 50 ° C no ka loaʻa ʻana o kahi keʻokeʻo wafer crude trifluoromethanesulfonamide me ka hua ʻaʻole i emi iho. 96% .